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The stability study was performed for the prepared formulation as per the ICH guidelines and it showed that the formulation F7 was stable, with no physical change and AJADD[1][4][2013]394‐412 also there was no significant reduction in drug From the FT-IR spectra, it was observed that similar characteristic peaks appear with minor differences for the drug and diltiazem their formulations .
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The DSC thermogram obtained for the pure drug, drug free beads and for the formulation shows that the drug was cardizem vs diltiazem diltiazem gtt diltiazem contraindications difference between diltiazem er and uniformly dispersed in an amorphous state in the polymer matrix .
diltiazem The SEM studies clearly showed that the obtained microcapsules exhibited good spherical nature .
The XRD studies are useful to investigate the crystallinity of the drugs after entrapment into the dosage forms; the x-ray diffraction studies indicated the amorphous diltiazem dispersion of the drug after entrapment into From the results of drug content determination, it can be inferred that there was a proper and uniform distribution of drug in the microcapsules prepared by Ionic encapsulation efficiency also showed that the drug loading is optimum .
The in vitro drug release indicated that the beads which were prepared with higher concentration diltiazem of Aluminium chloride released the drug more slowly .
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The increase in diltiazem initial drug loading increased the drug release .
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