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Though this reaction was simple and very good with respect to quality zolpidem and yield, but a larger amount of DCC urea by-product formation was observed hence, this process was not considered for scale up .
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Of the two reagents, PCl5 gave better yield and quality of the product and in case of SOCl2 the traces of un zolpidem reacted reagent must be removed from acid chloride reaction mass, otherwise it is affecting the quality of the product .
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